Description

2H–13C HETCOR MAS NMR is performed on 2H/13C/15N-Pro enriched A. aurantia dragline silk. Proline dynamics are extracted from 2H NMR line shapes and T1 in a site-specific manner to elucidate the backbone and side chain molecular dynamics for the MaSp2

2H–13C HETCOR MAS NMR is performed on 2H/13C/15N-Pro enriched A. aurantia dragline silk. Proline dynamics are extracted from 2H NMR line shapes and T1 in a site-specific manner to elucidate the backbone and side chain molecular dynamics for the MaSp2 GPGXX β-turn regions for spider dragline silk in the dry and wet, supercontracted states.

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    Title
    • Elucidating Proline Dynamics in Spider Dragline Silk Fibre Using 2H–13C HETCOR MAS NMR
    Contributors
    Date Created
    2014-03-24
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    Identifier
    • Digital object identifier: 10.1039/c4cc00971a
    • Identifier Type
      International standard serial number
      Identifier Value
      1359-7345
    Note
    • Link to published version: http://pubs.rsc.org/en/Content/ArticleLanding/2014/CC/c4cc00971a

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    This is a suggested citation. Consult the appropriate style guide for specific citation guidelines.

    Shi et al. Elucidating proline dynamics in spider dragline silk fibre using 2 H–13C HETCOR MAS NMR. ChemComm 2014, 50, 4856-4859 DOI:10.1039/c4cc00971a

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