Description
2H–13C HETCOR MAS NMR is performed on 2H/13C/15N-Pro enriched A. aurantia dragline silk. Proline dynamics are extracted from 2H NMR line shapes and T1 in a site-specific manner to elucidate the backbone and side chain molecular dynamics for the MaSp2 GPGXX β-turn regions for spider dragline silk in the dry and wet, supercontracted states.
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Title
- Elucidating Proline Dynamics in Spider Dragline Silk Fibre Using 2H–13C HETCOR MAS NMR
Contributors
Agent
- Shi, Xiangvan (Author)
- Yarger, Jeffrey (Author)
- Holland, Gregory (Author)
- College of Liberal Arts and Sciences (Contributor)
Date Created
The date the item was original created (prior to any relationship with the ASU Digital Repositories.)
2014-03-24
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Identifier
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Digital object identifier: 10.1039/c4cc00971a
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Identifier TypeInternational standard serial numberIdentifier Value1359-7345
Note
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Link to published version: http://pubs.rsc.org/en/Content/ArticleLanding/2014/CC/c4cc00971a
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Shi et al. Elucidating proline dynamics in spider dragline silk fibre using 2 H–13C HETCOR MAS NMR. ChemComm 2014, 50, 4856-4859 DOI:10.1039/c4cc00971a